The most appropriate procedure to demonstrate that matter is conserved during a chemical change or reaction is:
Find the mass of an acid and a base. Combine them to produce water and a salt. Find the mass of the water and salt.
This procedure involves a chemical reaction (neutralization reaction) where the reactants (acid and base) combine to form products (water and salt). By measuring the masses of the reactants before the reaction and the mass of the products after the reaction, you can demonstrate that the total mass remains constant, thus showing the conservation of matter.