The best procedure to demonstrate that matter is conserved during a chemical change or reaction is:
Find the mass of an acid and a base. Combine them to produce water and a salt. Find the mass of the water and salt.
This experiment shows a chemical change where two substances (the acid and base) react to form new substances (water and salt). Measuring the mass before and after the reaction allows you to demonstrate the conservation of mass, as the total mass should be the same before the reaction and after the products have formed.