The most appropriate question the scientist can answer with his experiment is:
b. Does increased activity lead to a higher volume of carbon dioxide produced?
This is because the experiment is designed to collect data specifically on the volume of gases produced during different levels of physical activity (running, walking, and resting). The focus on respiration and gas production (particularly carbon dioxide) directly relates to measuring the effects of increased physical activity. The other options involve comparisons or relationships that go beyond the data being collected.