Asked by loren

What effect would each of the following have on a sample'sobserved melting-point range ?

b.rapid heating
c.use of so much sample that the filled portion of the capillary tube extents considerably beyond the thermometer bulb
d.poor circulation of the heating bath liquid.
Answered by DrBob222
b. With rapid heating it is possible to shoot by the melting point.
c. I would expect a wider range.
d. inconsistent melting point form sample to sample.
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