Question
Posted by ann on Sunday, October 17, 2010 at 4:26am.
In melting point determination, why shouldn't a substance be re-melted? (i.e. why should we not re-melt a substance that has previously been melted in a melting point tube?)
In melting point determination, why shouldn't a substance be re-melted? (i.e. why should we not re-melt a substance that has previously been melted in a melting point tube?)
Answers
I think the original melting process may drive out some of the impurities in the sample and those condense in the upper part of the tube; therefore, taking the m.p. a second time means we are using a "different" sample. (But I've done that. ;-)]
Related Questions
In melting point determination, why shouldn't a substance be re-melted? (i.e. why should we not re-m...
After a Melting point determination, why can't you re-use the solidified substance and capllary tube...
If the melting point of a substance is -39C, has the substance melted at 20C?
How does melting order relate to melting point?
A. The substance that melted the quickest has the...