To separate a solid substance that has dissolved in water, you would use the method of boiling the water away, leaving the substance behind in the beaker. Therefore, the correct option is:
• Boil the water away, leaving the substance behind in the beaker.
This method works because when you boil the water, it evaporates, and any solid dissolved in it will be left in the beaker. The other options either won't work or are not appropriate for separating a dissolved solid.