The best procedure to demonstrate that matter is conserved during a chemical change or reaction is:
Find the mass of an acid and a base. Combine them to produce water and a salt. Find the mass of the water and salt.
This procedure involves a chemical reaction where new substances are formed (water and a salt) from the reactants (acid and base), and it allows you to demonstrate that the total mass of the reactants equals the total mass of the products, thereby illustrating the conservation of mass in a chemical reaction.